Laboratory Bharat Petroleum Corporation Ltd., QA

18. MS/HSD/SKO Sulphur, Total ASTM D4294 ISO 20847 0.0017% by Mass to 5.0% by Mass 19. MS Unwashed gum IS:1448 (Part 29) 1 ppm to 800 ppm 20. HSD Wate...

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Laboratory

Bharat Petroleum Corporation Ltd., QA Laboratory, Bhaunti, Kalpi Road, Panki, Kanpur, Uttar Pradesh

Accreditation Standard

ISO/IEC 17025: 2005

Certificate Number

TC-6432

Page 1 of 2

Validity

17.10.2017 to 16.10.2019

Last Amended on --

Sl.

Product / Material of Test

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

CHEMICAL TESTING I.

PETROLEUM AND PRODUCTS

1. 2. 3. 4. 5.

MS/HSD/SKO/MTO HSD SKO / MTO MS/HSD/SKO/MTO MS/HSD/SKO

Appearance Cetane Index, (Calculated) Colour Saybolt Colour Cu Strip Corrosion

6.

MS/HSD/SKO

Density

7.

MS/HSD/SKO

Distillation

WI-02 issue no.1 ASTM D-4737 IS:1448 (Part 14) Wi-03, Issue no.1 IS:1448 (Part 15)/2004 (Reaffirmed 2011) IS:1448 (Part 16) ASTM D1298 IS:1448 (Part 18) ASTM D-86

Temperature Recovery 8.

ETHANOL

9. 10.

MS MS

11.

SKO/HSD

12.

HSD

13. 14. 15.

HSD HSD ETHANOL

16.

MS

Iti Saxena Convenor

Ethanol Content at 15.6/15.6°C Ethanol Content Existent Gum

IS 15464

IS 2796 (Annexure E) IS:1448 (Part 29)/ 2004, (Reaffirmed 2011) Flash Point (Abel) IS:1448 (Part 20) IP 170 Kinematic Viscosity at 40°C IS:1448 (Part 25) ASTM D445 Kinematic Viscosity at 40°C IS: ASTM D7042/ 2014 Pour Point IS:1448 (Part 10) Relative Density at IS 15464 (Annexure-A) 15.6/15.6°C Research Octane No. IS:1448 (Part 27) / 2013 (RON) ASTM D2699 /2013b

Qualitative 40 to 60 0 to 30 units Qualitative (Visual) 1a units to 4c units 0.6600 g/ml to 1.000 g/ml

30°C to 400°C 0.1 % by vol. to 100 % by vol. 94 % by vol to 100 % by vol 0 to 20 % by vol 1.0 g/m3 to 100 g/m3 0 to 66°C 1.0 cSt to 400 cSt 1.0 cSt to 400 cSt (-)38 to 20 0.60 to 0.85 80 to 100

N. Venkateswaran Program Director

Laboratory

Bharat Petroleum Corporation Ltd., QA Laboratory, Bhaunti, Kalpi Road, Panki, Kanpur, Uttar Pradesh

Accreditation Standard

ISO/IEC 17025: 2005

Certificate Number

TC-6432

Page 2 of 2

Validity

17.10.2017 to 16.10.2019

Last Amended on --

Sl.

Product / Material of Test

Specific Test Performed

17. 18.

SKO MS/HSD/SKO

Smoke point Sulphur, Total

19. 20.

MS HSD

Unwashed gum Water Content

II.

LUBRICANTS

1.

Lubricants

Iti Saxena Convenor

Appearance Colour Colour ASTM

Test Method Specification against which tests are performed IS:1448 (Part 31) ASTM D4294 ISO 20847 IS:1448 (Part 29) IS:1448 (Part 40) /2010

WI-02 issue no.1 Wi-03, issue no.1 ASTM D: 1500 IS:1448 (Part 12) Crackle Test WI-03 A Issue no.1 Cu Strip Corrosion IS:1448 (Part 15)/ Density IS:1448 (Part 16) ASTM D1298/ 2012b Flash Point (COC) ASTM D : 92 IS:1448 (Part 69) Flash Point IS:1448 (Part 21) (Pensky Marten) ASTM D93/2012 Kinematic Viscosity IS:1448 (Part 25) /1976 at 40°C (Reaffirmed 2007) ASTM D445/ 2014 Kinematic Viscosity at 40°C IS: ASTM D7042/ 2014 Kinematic Viscosity at IS:1448 (Part 25)/ 1976 100°C (Reaffirmed 2007) ASTM D445/ 2014 Kinematic Viscosity at ASTM D7042 /2014 100°C Pour Point IS:1448 (Part 10)/ 2013 Viscosity Index ASTMD2270/2010e IS:1448 (Part 56)/ 2013 Water Content IS:1448 (Part 40)

Range of Testing / Limits of Detection 10 mm to 30 mm 0.0017% by Mass to 5.0% by Mass 1 ppm to 800 ppm 0 to 25 % by Vol.

Qualitative Qualitative (Visual) 0 to 5.0 units Qualitative (Visual) 1a unit to 4c unit 0.6600 g/ml to 1.000 g/ml 80°C to 400°C 66°C to 130°C 1.0 cSt to 400 cSt

1.0 cSt to 400 cSt 1.0 cSt to 50 cSt

1.0 cSt to 50 cSt (-)38 °C to 20°C NA 0 to 25% by Vol.

N. Venkateswaran Program Director