Laboratory Bharat Petroleum Corporation Ltd., Quality

Laboratory Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal Accredita...

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Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

1 of 8

S. No. Product / Material of Test

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

AT LABORATORY I.

PETROLEUM AND PRODUCTS

1.

ATF

2.

MS/ HSD/ SKO/ ATF/ SOLVENT/ ETHANOL/ HEXANE/ NAPHTHA/ LUBRICANTS

Ruchi Guntuku Convenor

Acidity, Total

IS 1448 (Part 113): 2011/ ASTM D-3242-11

0 to 0.100 mg KOH/g

API Gravity

IS 1571: 2008 (Table. 1)

30 to 60

Doctor Test

IS 1448 (Part 19): 1989 (RA 2013)

(+) ve to (–) ve

Electrical conductivity

IP 274-09/ ASTM D-2624-15

0 to 2000 pS/m

Freezing Point

IS 1448 (Part 11): 2004 (RA 2011)/ ASTM D 2386-15e1

(-) 70 °C to 0 °C

Kinematic Viscosity at (-20)°C

IS 1448 (Part 25): 1976 (RA 2013) / ASTM D445-12

1.0 cSt to 20 cSt

Naphthalene

IS 1448 (Part 118): 1985 (RA 2013)/ASTM D-1840-13

0 to 5% wt

Silver Strip Corrosion

IP 227-82

0 to 4 units

Appearance

WI-02a (Issue. 1 Dated. 01.10.2015)

Qualitative

N. Venkateswaran Program Manager

Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

2 of 8

S. No. Product / Material of Test 3.

ATF/SOLVENTS/ NAPHTHA/ MS

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

Aromatics

IS 1448 (Part 23): 2010/ ASTM D-1319-15

Aromatics: 5% to 60%

Olefins Content

Olefins : 0.3% to 55 %

4.

HSD/LDO/FO/LU BE

Ash Content

IS 1448 (Part 4): 2008 (RA 2013) ASTM D 482-13

0.001% to 1.0%

5.

MS

Benzene Content

ASTM D-3606-10

0.1% to 5.0%

Ethanol Content

IS 2796 (Annexure E)

0 to 20 %

Research Octane No.(RON)

IS 1448 (Part 27): 2013 / ASTM D2699-13b

40 to 100

6.

NAPTHA/FO

Calorific Value-Gross

IS 1448 (Part 7): 2004/ (RA 2011) / ASTM D 4868: 2010

9000 kcal/kg to 12000 kcal/kg

7.

HSD

Cetane Index

ASTM D 4737-10

1 to 65

8.

SKO/ SOLVENTS/ ATF

Colour Saybolt

IS 1448 (Part 14): 2008 (RA 2013) / ASTM D 156-15

(-)16 units to (+) 30 units

9.

MS/HSD/SKO

Colour

WI-03 (Issue. 1 Dated. 01.10.2015)

Qualitative (Visual)

10.

MS/HSD/SKO/ LDO/ ATF/SOLVENTS/ LUBRICANTS

Cu Strip Corrosion

IS 1448 (Part 15): 2004 (RA 2011) ASTM D-130-12

1 a unit to 4 c unit

Ruchi Guntuku Convenor

N. Venkateswaran Program Manager

Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

3 of 8

S. No. Product / Material of Test 11.

12.

GREASE

FO

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

Consistency of worked Grease at 25 (±) 0.5°C

IS 1448 (Part 60): 1994 (RA 2011) ASTM D-217-10

85units to 475 units

Drop point

IS 1448 (Part 52): 1971 (RA 2013)

30 ºC to 230 ºC

ASTM D 2265- 2015

30 ºC to 280 ºC

Condarson Carbon Residue

IS 1447 (Part 122): 2013

0.01%b to 30%

Kinematic Viscosity at 50°C

IS 1448 (Part 25): 1976 (RA 2013) / ASTM D445-15

1.0 cSt to 400 cSt

0.660 g/ml to 1.00 g/ml Or 660.0 kg/m3 to 1000.0 kg/m3

13.

MS/HSD/SKO/ LDO/FO/SOLVE NTS/ATF/ NAPTHA/ LUBRICANT

Density

IS 1448 (Part 16): 1990 (RA 2014) / ASTM D1298-12b ASTM D 4052-11

14.

MS/HSD/SKO/ ATF/ SOLVENT/MTO/ NAPTHA

Distillation

IS 1448 (Part 18): 1991 (RA 2010)/ ASTM D-86-15

15.

ETHANOL

Ruchi Guntuku Convenor

Temperature

30°C to 400°C

Volume Recovery

5 % to 99 %

Ethanol Content at 15.6/15.6°C

IS 15464: 2004

94 % to 100 %

Miscibility with Water

IS 15464: 2004 (Annexure C)

Qualitative (Yes/No)

Relative Density at 15.6/15.6°C

IS 15464: 2004 (Annexure A)

0.60 to 0.85

N. Venkateswaran Program Manager

Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

4 of 8

S. No. Product / Material of Test 16.

MS/ATF

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

Existent Gum

IS 1448 (Part 29): 2004 (RA 2011) / ASTM D-381-12

1.0 to 100

Water Reaction

IS 1448 (Part 42) 1977 (RA 2011) / ASTM D1094-07(2013)

Interface rating Separation Rating

0 to 4 units 1 units to 3 units

1 7.

HFHSD/LDO/FO/ LUBRICANTS

Flash Point (Pensky Marten)

IS 1448 (Part 21): 2012/ ASTM D93-15

40°C to 350°C

18.

HSD/SKO/MTO/ ATF

Flash Point (Abel)

IS 1448 (Part 20): 1998 (RA 2013) /IP 170-14

(-)19 °C to (+)70 °C

19.

HSD/LDO/FO

Sediments

IS 1448 (Part 30): 2013 ASTM D-473-07: (2012)

0 to 10 %

20.

LUBRICANTS/ HSD/ LDO

Kinematic Viscosity at 40°C

IS 1448 (Part 25): 1976 (RA 2013) / ASTM D445-15

1.0 cSt to 1200 cSt

ASTM D 7042-14

1.0 cSt to 400 cSt

Pour Point

IS 1448 (Part 10): 2013 / ASTM D 97-15

(-)39 °C to (+)50°C

22.

ATF/SKO

Smoke point

IS 1448 (Part 31): 1968/ (RA 2013) ISO 3014: 1993/ ASTM D-1322-15e1

5mm to 35mm

23.

MS/HSD/SKO/ LDO/FO/ATF/ NAPTHA

Sulphur, Total

ASTM D 4294: 10/ IP 336: 04

0.0005% to 5.0% Or 5ppm to 5000 ppm

Ruchi Guntuku Convenor

N. Venkateswaran Program Manager

Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

5 of 8

S. No. Product / Material of Test

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

24

MS/HSD

Sulphur, Total

ISO 20847: 04

0 to 500%

25.

MS/HSD/FO

Sulphur, Total

ASTM:D7220: 12

0.0005% to 5.0%

26

HSD/LDO/FO/ LUBRICANTS

Water Content

IS 1448 (Part 40): 1987 (RA 2011) / ASTM D-95-13e1

0 to 25%

II.

LUBRICANTS

1.

Lubricants

Foaming Characteristics

ASTM D892-13

0 to 500 units

Frothing Test

IS 1448 (Part 99): 1981 (RA 2013)

0 to 30 ml

Flash Point (COC)

ASTM D 92-12b/ IS 1448 (Part 69): 2013

40°C to 380°C

Colour ASTM

ASTM D 1500-12 / IS 1448 (Part 12): 2013

0 to 8.0 units

Insoluble (Pentane & Toluene)

ASTM D893-12

0.01 to 1.0 %

Crackle Test

WI-02A (Issue. 1 Dated. 01.10.2015)

Qualitative

Emulsion Characteristics

ASTM D1401-12e1

0 to 30 minute

Emulsion Stability Test

IS 1448 (Part 98): 1981 (RA 2013)

0 to 0.2 ml

Total Base Number (TBN)

ASTM D 2896-11/ IS 1448 (Part 86): 1977 (RA 2011)

0.1 mg KOH/gm to 40.0 mg KOH/gm

Ruchi Guntuku Convenor

N. Venkateswaran Program Manager

Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

6 of 8

S. No. Product / Material of Test Lubricants

Ruchi Guntuku Convenor

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

Viscosity Index

ASTM D 2270-10e1/ IS 1448 (Part 56): 2013 ASTM:D7042-14

85 to 150

Total Acid Number (TAN)

ASTM D 664-11a/ IS 1448 (Part 1 ): 2002 (RA 2013)

0.1 mg KOH/gm to 40.0 mg KOH/gm

Kinematic Viscosity at 100°C

IS 1448 (Part 25): 1976 (RA 2013) / ASTM D445-15

1.0 cSt to 25.0 cSt

Kinematic Viscosity at 100 °C

ASTM D 7042-14

1.0 cSt to 400 cSt

N. Venkateswaran Program Manager

Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

7 of 8

S. No. Product / Material of Test

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

AT MOBILE LABORATORY I.

PETROLEUM AND PRODUCTS

1.

MS/HSD/ LUBRICANTS

Appearance

WI-02a (Issue No. I dated 01.10.2015)

Qualitative (Visual)

Density

IS 1448 (Part 16): 1990 (RA 2013) /ASTM D1298-12

650-1000 Kg/m3 0.650-1.000 gm/ml Qualitative (Visual)

2.

MS/HSD/SKO

Colour

WI-03 (Issue No. I dated 01.10.2015)

3.

MS/HSD

Distillation

IS 1448 (Part 18): 1991 (RA 2006 / ASTM D-86-15

IBP FBP Volume recovered

30 °C to 400 °C

5 % Vol. to 99 % Vol.

Sulphur

IP 336-04 IS 1448 (Part 153): 2012 / ASTM D 4294-10

5 ppm to 500 ppm

4.

HSD

Flash Point (Abel)

IS 1448 (Part 20): 1998 (RA 2013) IP 170- 2014

(-) 19 to (+)70 °C

5.

LUBRICANTS/ HSD

Kinematic Viscosity at 40°C

IS 1448 (Part 25) (RA 2013) ASTM D 445 -15 ASTM D 7042-14

1.0 cSt to 700 cst

II.

LUBRICANTS

1.

Lubricants

Viscosity Index

ASTM D 2270-10 e1 / IS 1448 (Part 56): 2013

85 to 150

Additive elements Ca & Zn

ASTM D-6481-14

0.002 % to 0.60 % mass

Ruchi Guntuku Convenor

N. Venkateswaran Program Manager

Laboratory

Bharat Petroleum Corporation Ltd., Quality Assurance Laboratory, Budge Budge Installation, P.O. Budge Budge, Kolkata, West Bengal

Accreditation Standard

ISO/IEC 17025: 2005

Discipline

Chemical Testing

Issue Date

23.04.2016

Certificate Number

T-0841

Valid Until

22.04.2018

Last Amended on

-

Page

8 of 8

S. No. Product / Material of Test Lubricants

Specific Test Performed

Test Method Specification against which tests are performed

Range of Testing / Limits of Detection

Flash point (COC)

ASTM D 92-2012b / IS 1448 (Part 69): 2013

40 °C to 380 °C

Water By Distillation

IS 1448 (Part 40): 1987 (RA 2010)/ASTM D 95-2013 e1

0 to 25 % Vol.

Kinematic Viscosity at 100 °C

IS 1448 (Part 25): 1976 (RA 2013)/ ASTM D 445 -15

1.0 cSt to 20 cSt

Crackle Test

WI-02A (Issue No. I, dated 01.10.2015)

Qualitative

-X-X-X-X-X-X-X-X-X-X-X-X-X-X-

Ruchi Guntuku Convenor

N. Venkateswaran Program Manager